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JOURNAL OF SYNTHETIC CRYSTALS ›› 2024, Vol. 53 ›› Issue (11): 1990-1996.

Special Issue: 高功率激光用晶体和透明陶瓷

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Influence of Acid-Washing Treatment of Y2O3 Nanopowder on the Optical Properties of Transparent Ceramics

LIU Xiaolong1, FU Zhongchao1, WU Nan1, LONG Haibo1, SHAO Cen2,3, REN Yi4, HOU Zhaoxia1, ZHANG Le2,3   

  1. 1. School of Mechanical Engineering, Shenyang University, Shenyang 110044, China;
    2. School of Physics Electronic Engineering, Jiangsu Normal University, Xuzhou 221116, China;
    3. Jiangsu Xiyi Advanced Materials Research Institute of Industrial Technology, Xuzhou 221400, China;
    4. Fujian Golden Dragon Rare-Earth Co., Ltd., Longyan 366300, China
  • Received:2024-09-10 Online:2024-11-15 Published:2024-12-09

Abstract: Y2O3 transparent ceramics have broad applications including solid-state lasers, transparent windows, etc., owing to its excellent optical and physical-chemical properties. The dispersity of the powder among the fabrication process of transparent ceramics has attracted much attention from researchers for decades. In this paper, domestic commercial nanopowder was adopted as the starting material, and the dispersion of the powder was improved through mechanical force combined with HF acid-washing. Y2O3 transparent ceramics with high transmittance were achieved by slip casting and vacuum sintering. The results show that ultrasonic combined with HF acid-washing is an effective way to improve the dispersibility and sinterability of the powder, the D50 of the powder reduces from 3.5 μm to 1.4 μm. The transmittance of the Y2O3 ceramic at 400 nm is improved from 65.5% to 71.5% for the sample after ultrasonic combined with HF acid-washing process. The results lay a solid foundation of preparation technology and theoretical basis for the application of Y2O3 transparent ceramics on solid-state lasers and transparent window materials.

Key words: Y2O3, powder, dispersity, acid-washing, transparent ceramics, sintering

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