摘要： 在室温和无溶剂研磨条件下,氯化锌催化1,3-二苯基-4-甲酰基吡唑与4-氨基安替比林反应生成新型席夫碱,收率84;.并对其进行X-射线单晶衍射、元素分析、红外光谱、热重分析表征.X-射线单晶衍射结果表明:该晶体为单斜晶系,空间群P21/n,a=1.63310(18) nm,b =0.79964(9) nm,c=1.84620(2) nm,β=100.554(10)°,V=2.3701(5) nm3,Z=4,dC=1.215 g/em3,μ=0.077 mm-1,F(000)=912.
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王俊岭;吴峰敏;汪小伟;马军营. 新型吡唑Schiff碱的固相合成与晶体结构[J]. 人工晶体学报, 2014, 43(11): 3027-3032.
WANG Jun-ling;WU Feng-min;WANG Xiao-wei;MA Jun-ying. Solid-phase Synthesis and Crystal Structure of a Novel Pyrazole Schiff Base by Solid Phase Method[J]. JOURNAL OF SYNTHETIC CRYSTALS, 2014, 43(11): 3027-3032.
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