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人工晶体学报 ›› 2007, Vol. 36 ›› Issue (5): 1118-1122.

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碳化气体引入温度对3C-SiC薄膜生长的影响

郑海务;郭凤丽;苏剑峰;顾玉宗;张华荣;傅竹西   

  1. 河南大学物理与电子学院,微系统物理研究所,开封,475004;中国科学技术大学物理系,合肥,230026;河南大学物理与电子学院,微系统物理研究所,开封,475004;中国科学技术大学物理系,合肥,230026
  • 出版日期:2007-10-15 发布日期:2021-01-20
  • 基金资助:
    国家自然科学基金(50532070;50472009;90201038;10474091);Foundation of Scientific Research of Henan University(06YBZR022)

Influence of Temperature of Carbonization Gas Introduction on the Growth of 3C-SiC films

ZHENG Hai-wu;GUO Feng-li;SU Jian-feng;GU Yu-zong;ZHANG Hua-rong;FU Zhu-xi   

  • Online:2007-10-15 Published:2021-01-20

摘要: 通过低压化学气相沉积方法,在Si(100)衬底上生长了高度择优取向的3C-SiC(100)薄膜.SiC(200)峰的摇摆曲线表明SiC薄膜的结晶质量随着丙烷气体引入温度(Tgi)的升高而增加.选区电子衍射像表明高Tgi下生长的薄膜比低Tgi下生长的薄膜具有更好的取向.典型的SiC薄膜高分辨像中观察到了孪晶和层错.表面场发射扫描电镜像表明随着Tgi的升高,SiC薄膜的表明形貌发生了改变.

关键词: 3C-SiC薄膜;微结构;表面形貌

Abstract: 3C-SiC(100)films with preferred orientation were grown on Si (100) substrates by low-pressure chemical vapor deposition (LPCVD). The rocking curves of the SiC (200) peaks show that the crystalline quality of the films is improved with increasing temperature of propane introduction (abbreviated Tgi). Representative Selected area electron diffraction (SAED) patterns show that the film carbonized at higher Tgi has more preferable orientation than that carbonized at relatively low Tgi. Defects (stacking faults) were observed through the typical high resolution transmitted electron microscopy (HRTEM) image in the film. Field emission scanning electron microscopy (FESEM) images indicate that the surface morphologies of the films vary with increasing Tgi.

Key words: 3C-SiC(100)films with preferred orientation were grown on Si (100) substrates by low-pressure chemical vapor deposition (LPCVD). The rocking curves of the SiC (200) peaks show that the crystalline quality of the films is improved with increasing temperature of propane introduction (abbreviated Tgi). Representative Selected area electron diffraction (SAED) patterns show that the film carbonized at higher Tgi has more preferable orientation than that carbonized at relatively low Tgi. Defects (stacking faults) were observed through the typical high resolution transmitted electron microscopy (HRTEM) image in the film. Field emission scanning electron microscopy (FESEM) images indicate that the surface morphologies of the films vary with increasing Tgi.

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