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人工晶体学报 ›› 2021, Vol. 50 ›› Issue (7): 1391-1396.

• 研究论文 • 上一篇    

Sm∶YAG/Sm∶Y3ScAl4O12单晶光纤的生长及光谱性能

徐杰1, 宋青松2, 刘坚2, 丁雨憧3, 李东振1, 徐晓东1, 徐军2   

  1. 1.江苏师范大学物理与电子工程学院,徐州 221116;
    2.同济大学物理科学与工程学院,上海 200092;
    3.中国电子科技集团第二十六研究所,重庆 400060
  • 收稿日期:2021-05-06 出版日期:2021-07-15 发布日期:2021-08-16
  • 通讯作者: 徐晓东,博士,教授。E-mail:xdxu79@jsnu.edu.cn;徐军,博士,教授。E-mail:xujun@mail.shcnc.ac.cn
  • 作者简介:徐杰(1990—),男,安徽省人。E-mail:535000689@qq.com
  • 基金资助:
    国家自然科学基金(61621001)

Growth and Spectral Properties of Sm3+-Doped YAG and Y3ScAl4O12 Single Crystal Fibers

XU Jie1, SONG Qingsong2, LIU Jian2, DING Yuchong3, LI Dongzhen1, XU Xiaodong1, XU Jun2   

  1. 1. School of Physics and Electronic Engineering, Jiangsu Normal University, Xuzhou 221116, China;
    2. School of Physics Science and Engineering, Tongji University, Shanghai 200092, China;
    3. The 26th Research Institute, China Electronics Technology Group Corporation, Chongqing 400060, China
  • Received:2021-05-06 Online:2021-07-15 Published:2021-08-16

摘要: 采用微下拉法成功生长出Sm∶YAG和Sm∶Y3ScAl4O12单晶光纤。XRD结果表明晶体为立方晶系,晶胞参数分别为a=1.199 3 nm和a=1.200 0 nm。测试了室温下单晶光纤的拉曼光谱、吸收光谱、荧光光谱和荧光寿命。Sm∶Y3ScAl4O12最大声子能量为766 cm-1。Sm∶YAG和Sm∶Y3ScAl4O12 在可见波段的最强吸收位于405 nm附近,非常适合InGaN/GaN二极管泵浦。404 nm激发下,最强发射带位于618 nm处, 对应于Sm3+4G5/26H7/2能级跃迁, 测得Sm∶YAG和Sm∶Y3ScAl4O12上能级4G5/2的荧光寿命分别为1.86 ms和1.83 ms。实验结果表明Sm∶YAG和Sm∶Y3ScAl4O12单晶光纤是有潜力的红橙光波段激光增益介质。

关键词: Sm∶YAG, Sm∶Y3ScAl4O12, 单晶光纤, 微下拉法, 晶体生长, 可见激光, 光谱性能

Abstract: Sm3+-doped YAG and Y3ScAl4O12 single crystal fibers were successfully grown by the micro-pulling-down (μ-PD) technique. X-ray diffraction test shows that the crystals are cubic phase structure, the lattice constants of Sm∶YAG and Sm∶Y3ScAl4O12 single crystal fibers are calculated to be a=1.199 3 nm and a=1.200 0 nm, respectively. The Raman spectra, absorption spectra, fluorescence spectra and fluorescence lifetimes of the crystal fibers were measured at room temperature. The strong absorption band centered at 405 nm matches well the InGaN/GaN laser diode pumping. Under 404 nm excitation, the emission transition of 4G5/26H7/2 peaked at 618 nm appears to be strongest, and the fluorescence lifetime of the 4G5/2 level of Sm3+-doped YAG and Y3ScAl4O12 single crystal fibers are determined to be 1.86 ms and 1.83 ms, respectively. The experimental data shows that Sm∶YAG and Sm∶Y3ScAl4O12 single crystal fibers are potential laser media in the red-orange wavelength range.

Key words: Sm∶YAG, Sm∶Y3ScAl4O12, single crystal fiber, micro-pulling-down method, crystal growth, visible laser, spectral property

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