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人工晶体学报 ›› 2017, Vol. 46 ›› Issue (2): 193-196.

• • 上一篇    下一篇

导模法生长高质量氧化镓单晶的研究

贾志泰;穆文祥;尹延如;张健;陶绪堂   

  1. 山东大学晶体材料国家重点实验室,济南250100;中山大学光电材料与技术国家重点实验室,广州510275;山东大学晶体材料国家重点实验室,济南,250100
  • 出版日期:2017-02-15 发布日期:2021-01-20
  • 基金资助:
    山东大学青年学者未来计划(2015WLJH36);光电材料与技术国家重点实验室开放课题(OEMT-2015-KF-06)

Growth of High Quality β-Ga2O3 Single Crystal by EFG Method

JIA Zhi-tai;MU Wen-xiang;YIN Yan-ru;ZHANG Jian;TAO Xu-tang   

  • Online:2017-02-15 Published:2021-01-20

摘要: 使用导模法生长了宽度25 mm,长度100 mm的氧化镓(β-Ga2O3)单晶.晶体外观完整、无色、无开裂,粉末XRD测试证明所获得的晶体为β相,晶体摇摆曲线半峰宽为93.6",峰形对称,说明晶体质量良好.测试了未掺杂晶体的紫外透过光谱,并推算了晶体的禁带宽度为4.77 eV.此外,还重点讨论了晶体放肩时的工艺参数对晶体质量的影响.

关键词: 氧化镓单晶;导模法;禁带宽度

Abstract: High quality β-Ga2O3 single crystal with 25 mm in width and 100 mm in length were grown by edge-defined film-fed growth (EFG) method.The crystal apperance complete,colorless,no cracking.Powder X-ray diffraction demonstrated that the obtained crystal is β phase.High-resolution X-ray diffraction showed a full-width at half-maximum (FWHM) of the rocking curve of 93.6",indicating a high crystal quality.The ultraviolet absorption spectrum was investigated and the bandgap was estimated to be 4.77 eV.Furthermore,the effect of shouldering processing parameters on crystal quality was also discussed.

Key words: High quality β-Ga2O3 single crystal with 25 mm in width and 100 mm in length were grown by edge-defined film-fed growth (EFG) method.The crystal apperance complete,colorless,no cracking.Powder X-ray diffraction demonstrated that the obtained crystal is β phase.High-resolution X-ray diffraction showed a full-width at half-maximum (FWHM) of the rocking curve of 93.6",indicating a high crystal quality.The ultraviolet absorption spectrum was investigated and the bandgap was estimated to be 4.77 eV.Furthermore,the effect of shouldering processing parameters on crystal quality was also discussed.

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