Synthesis and Crystal Structure Characterization of 3,5-dichloro Salicylaldehyde Isoleucine Phenanthroline Copper(Ⅱ)Ternary Complex

Abstract

Abstract: The 3,5-dichloro salicylaldehyde isoleucine phenanthroline copper(Ⅱ)ternary complex was composed in step-by-step method in alkaline solution,and the single crystal[Cu3L3(Phen)3].5H2O(H2L=2-[(3,5-Dichloro-2-hydroxy-benzylidene)-amino]-3-methyl-pentanoic acid)was determined from the ternary complex.The structure of the single crystal has been characterized by elemental analysis,IR and X-ray single crystal diffraction.

Key words: The 3,5-dichloro salicylaldehyde isoleucine phenanthroline copper(Ⅱ)ternary complex was composed in step-by-step method in alkaline solution,and the single crystal[Cu3L3(Phen)3].5H2O(H2L=2-[(3,5-Dichloro-2-hydroxy-benzylidene)-amino]-3-methyl-pentanoic acid)was determined from the ternary complex.The structure of the single crystal has been characterized by elemental analysis,IR and X-ray single crystal diffraction.

CLC Number:

LIU Zheng;XIA Jin-hong;WANG Yong-liao;WEI Chun. Synthesis and Crystal Structure Characterization of 3,5-dichloro Salicylaldehyde Isoleucine Phenanthroline Copper(Ⅱ)Ternary Complex[J]. Journal of Synthetic Crystals, 2008, 37(6): 1542-1545.

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Synthesis and Crystal Structure Characterization of 3,5-dichloro Salicylaldehyde Isoleucine Phenanthroline Copper(Ⅱ)Ternary Complex

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