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JOURNAL OF SYNTHETIC CRYSTALS ›› 2017, Vol. 46 ›› Issue (5): 890-896.

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Process Parameters Optimization of Micro/Nano-crystalline CVD Diamond Coatings

XU Chen-yang;XIE Ya-juan;DENG Fu-ming;CHEN Li;LEI Qing   

  • Online:2017-05-15 Published:2021-01-20

Abstract: The process parameters were designed by orthogonal experiment.Diamond coatings were synthesized by Hot Filament Chemical Vapor Deposition (HFCVD) and the scanning electron microscopy (SEM), rockwell hardness tester, X-ray diffraction (XRD) were used to test the coating properties and cutting tests to determine the optimum carbon source concentration, deposition pressure and hot wire/substrate spacing for the micro and nano layers.The results show that the optimum micro-diamond coating deposition process parameters are carbon source concentration of 2;, deposition pressure 3 kPa, hot wire/substrate spacing 5 mm.The optimum nano-diamond coating deposition process parameters are Carbon source concentration of 5;, deposition pressure 5 kPa, hot wire/substrate spacing 8 mm.

Key words: The process parameters were designed by orthogonal experiment.Diamond coatings were synthesized by Hot Filament Chemical Vapor Deposition (HFCVD) and the scanning electron microscopy (SEM), rockwell hardness tester, X-ray diffraction (XRD) were used to test the coating properties and cutting tests to determine the optimum carbon source concentration, deposition pressure and hot wire/substrate spacing for the micro and nano layers.The results show that the optimum micro-diamond coating deposition process parameters are carbon source concentration of 2;, deposition pressure 3 kPa, hot wire/substrate spacing 5 mm.The optimum nano-diamond coating deposition process parameters are Carbon source concentration of 5;, deposition pressure 5 kPa, hot wire/substrate spacing 8 mm.

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